NMR – from Spectra to Structures – an Experimental Approach, 2nd Edition by N. Mitchell and Costisella : Our attempt to present NMR spectroscopy to the beginner in a somewhat different way was well-received, so that we were invited by Springer to make some additions to the original for a second edition. Naturally we have modified the text to take account of justified criticisms of the first edition. We decided immediately to extend the number and scope of the problems section comprising Part 2, as we know that this section has been very useful to our readers. We felt that solid-state NMR is now so important and so relatively easy to do that it would be well worth giving the reader a brief account of its advantages and disadvantages. And, having already dealt with four important nuclei in some detail, we decided to add some basic information on a number of other spin-½ nuclei which are now often studied. We thank Prof. Janet Blümel, Texas A&M University, and the Gesellschaft Deutscher Chemiker for allowing us to reproduce solid state NMR spectra. In addition we thank Klaus Jurkschat and Bernhard Lippert and their groups for making available samples of organometallic molecules. Thanks also go to Andrea Bokelmann and Bernhard Griewel for their valuable technical help.

NMR – from Spectra to Structures – an Experimental Approach, 2nd Edition by N. Mitchell and Costisella

Title: NMR – from Spectra to Structures – an Experimental Approach
Editor: Terence N. Mitchell
Burkhard Costisella
Edition: 2nd, Revised, Expanded
Publisher: Springer Publications
Length: 220 pages
Size: 4.56 MB
Language: English

 

This practice-oriented textbook shows how to utilize the huge variety of NMR experiments available today in addition to standard experiments. Intended as a practical guide for students and laboratory personnel, it treats theoretical aspects only to the extent necessary to understand the experiments and to interpret the results. The book is significantly revised and expanded for the 2nd edition, and now includes the nuclei 1H/2H, 13C, 31P, 17O, 15N, 19F, 29Si, 77Se, 113Cd, 117Sn/119Sn, 195Pt, 207Pb and a new chapter on solid state NMR. An expanded set of 50 graded problems offers invaluable help for students, practitioners and laboratory personnel alike.

Solutions Manual NMR from spectra to structures: an experimental approach

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NMR – from spectra to structures: an experimental approach

Author(s): Terence N. Mitchell, Burkhard Costisella

Publisher: Springer, Year: 2007

ISBN: 3540721959

 

[PDF] NMR – from Spectra to Structures – an Experimental Approach by N. Mitchell and Costisella Table Of Contents

Front Matter….Pages I-XIII
Introduction….Pages 1-2
1D Experiments….Pages 3-39
2D Experiments….Pages 39-51
Quadrupolar Nucleus Experiments….Pages 51-53
HPLC-NMR Coupling….Pages 53-59
Other Spin-1/2 Nuclei….Pages 59-72
Solid State NMR….Pages 73-83
Back Matter….Pages 84-84
Section 1….Pages 85-88
Worked Example….Pages 88-91
Problems….Pages 93-163
Section 2….Pages 164-207


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